Highly Sensitive and Selective Formaldehyde Gas Sensors Based on Polyvinylpyrrolidone/Nitrogen-Doped Double-Walled Carbon Nanotubes

Author(s)
Thanattha Chobsilp, Thotsaphon Threrujirapapong, Visittapong Yordsri, Alongkot Treetong, Saowaluk Inpaeng, Karaked Tedsree, Paola Ayala, Thomas Pichler, Lei Shi, Worawut Muangrat
Abstract

A highly sensitive and selective formaldehyde sensor was successfully fabricated using hybrid materials of nitrogen-doped double-walled carbon nanotubes (N-DWCNTs) and polyvinylpyrrolidone (PVP). Double-walled carbon nanotubes (DWCNTs) and N-DWCNTs were produced by high-vacuum chemical vapor deposition using ethanol and benzylamine, respectively. Purified DWCNTs and N-DWCNTs were dropped separately onto the sensing substrate. PVP was then dropped onto pre-dropped DWCNT and N-DWCNTs (hereafter referred to as PVP/DWCNTs and PVP/N-DWCNTs, respectively). As-fabricated sensors were used to find 1,2-dichloroethane, dichloromethane, formaldehyde and toluene vapors in parts per million (ppm) at room temperature for detection measurement. The sensor response of N-DWCNTs, PVP/DWCNTs and PVP/N-DWCNTs sensors show a high response to formaldehyde but a low response to 1,2-dichloroethane, dichloromethane and toluene. Remarkably, PVP/N-DWCNTs sensors respond sensitively and selectively towards formaldehyde vapor, which is 15 times higher than when using DWCNTs sensors. This improvement could be attributed to the synergistic effect of the polymer swelling and nitrogen-sites in the N-DWCNTs. The limit of detection (LOD) of PVP/N-DWCNTs was 15 ppm, which is 34-fold higher than when using DWCNTs with a LOD of 506 ppm. This study demonstrated the high sensitivity and selectivity for formaldehyde-sensing applications of high-performance PVP/N-DWCNTs hybrid materials.

Organisation(s)
Electronic Properties of Materials
External organisation(s)
Burapha University, King Mongkut's University of Technology Thonburi, National Metal and Materials Technology Center (MTEC), National Science and Technology Development Agency, Sun Yat-sen University
Journal
Sensors
Volume
22
No. of pages
10
ISSN
1424-8220
DOI
https://doi.org/10.3390/s22239329
Publication date
12-2022
Peer reviewed
Yes
Austrian Fields of Science 2012
103018 Materials physics
Keywords
ASJC Scopus subject areas
Analytical Chemistry, Information Systems, Instrumentation, Atomic and Molecular Physics, and Optics, Electrical and Electronic Engineering, Biochemistry
Portal url
https://ucrisportal.univie.ac.at/en/publications/9e6b150c-d22f-45e4-b47a-2942b68d19bf